UNF Department of Chemistry - Analytical Services

Dr. Nelson Zhao Instrumentation Facility Manager Phone: (904) 620-1962 E-mail: nelson.zhao@unf.edu

The Analytical Instrumentation Facility houses a number of advanced analytical instruments which can be used to analyze numerous samples for you. Our instruments include NMR, FTIR (Solid and Liquid), UV-Vis, AA, GC, GC/MS, and XRD.

 

Our services are available at reasonable prices. Whether it is a simple sample analysis, method development, or a more complicated structural elucidation, quality work is provided in a timely fashion.

 

Click the instrument below for rate information. The charges are on a per sample or per hour basis depending on the instrument involved. For special requests such as NMR data interpretations, analyses requiring the use of several instruments, complex mixture analysis, etc., please contact Nelson Zhao at (904) 620-1962 or by email at nelson.zhao@unf.edu

• Nuclear Magnetic Resonance Analysis (NMR)

  The NMR lab is equipped with a Agilent VNMRS 500 MHz Nuclear Magnetic Resonance instrument.

  Solution Probes:

  • ¹H-¹⁹F/¹⁵N-³¹P 5 mm PFG AutoX Dual Broadband Probe for ¹H, ¹⁹F, as well as other nuclei in the resonance frequency range between 50 MHz (¹⁵N) and 202 MHz (³¹P).
  • ¹H-¹⁹F{¹³C} 5mm Triple resonance PFG probe; indirect detection with high sensitivity for ¹H and ¹⁹F.

  Both probes have VT capability between -80°C and +120°C. In addition to 1D ¹H, ¹⁹F, ¹³C, ³¹P, ²⁹Si NMR experiments, the instrument can acquire APT, DEPT, and 2D experiments such as COSY, TOCSY, NOESY, HSQC, and HMBC.

  Rates (per sample)

  Charge per sample	On Campus	Off Campus (academic)	Industry
  1H	$25	$40	$60
  13C/29Si	$40	$55	$90
  19F	$25	$40	$60
  31P	$40	$55	$90
  APT	$40	$60	$90
  DEPT	$50	$70	$100
  COSY	$40	$60	$80
  TOCSY	$50	$70	$100
  HSQC	$60	$100	$120
  HMBC	$100	$150	$170

  Solid State NMR - Please inquire

• Infrared Spectroscopy (FTIR)

  Available Instruments:

  • Perkin-Elmer Spectrum BX (with liquid attenuated total reflectance (ATR) accessory)
  • Perkin-Elmer Spectrum One (with solid attenuated total reflectance (ATR) accessory)
  • Shimadzu IRAffinity-1 FTIR

  IR Service Rates (per sample)

  	On Campus	Off Campus (academic)	Industry
  Charge per sample	$25	$40	$60

   

  

  Perkin Elmer Spectrum One FTIR

  

  Perkin Elmer Spectrum BX FTIR

• Ultraviolet and Visible Spectroscopy (UV/Vis)

  Perkin-Elmer Lambda 35 UV-Visible spectrophotometer can be used to perform quantitation, spectral scans, and kinetic analysis in the ultraviolet (UV) to visible wavelength range (190 - 850 nm).

  Rates*

  	On Campus	Off Campus (academic)	Industry
  Charge per hour	$40	$60	$80

  *minimum charge is 1 hour

   

  

  Perkin Elmer Lambda 35 UV-Vis

• Atomic Absorption Analysis (AA)

  The department is equipped with a Perkin Elmer AAnalyst 800 instrument for metals analysis. There are many Hollow Cathode Lamps (HCL) and Electrodeless Discharge Lamps (EDL) ready for metal ion analyses. They include Calcium, Iron, Magnesium, Manganese, Copper, Aluminum, Chromium, Zinc, Lead, Antimony, Cadmium, Selenium, Tin, and Arsenic. Please call Nelson Zhao at (904)620-1962 or by email at nelson.zhao@unf.edu for other metal analyses.

  Rates^*

  	On Campus	Off Campus (academic)	Industry
  Charge per hour	$40	$60	$80

  *minimum charge is 1 hour

   

  

  Perkin Elmer AAnalyst 800 AA

• Gas Chromatographic Analysis (GC)

  Available Instruments:

  • Perkin Elmer Clarus 500 GC with FID
  • Agilent HP5890 GC with FID/ECD (dual column option)

  Rates*

  	On Campus	Off Campus (academic)	Industry
  Charge per hour	$40	$60	$80

  *minimum charge is 1 hour

  If method development is required, please contact Nelson Zhao at (904) 620-1962 or by email at nelson.zhao@unf.edu for rates.

   

  

  Perkin Elmer Clarus 500GC

• Gas Chromatograph-Mass Spectrometric Analysis (GC-MS)

  Available Instruments:

  • Varian CP-3800 GC and Saturn 2200 GC/MS system
  • Agilent HP5890 GC and HP5972 MS system

  Rates*

  	On Campus	Off Campus (academic)	Industry
  Charge per hour	$40	$60	$80

  *minimum charge is 1 hour

  If method development is required, please contact Nelson Zhao at (904) 620-1962 or by email at nelson.zhao@unf.edu for quotes.

   

  

  Varian CP-3800 and Saturn 2200 GC/Ms

• Powder X-Ray Diffraction (XRD)

  Available Instruments:

  • Rigaku Ultima III Powder Diffractometer

  Rates*

  	On Campus	Off Campus (academic)	Industry
  Charge per hour	$40	$60	$80

  *minimum charge is 1 hour

• Quanta Master 30 PTI Spectrofluorometer

  Available Instruments:

  • Quanta Master 30 PTI Spectrofluorometer with high-power Xe flash lamp

  Rates:

  	On Campus	Off Campus (academic)	Industry
  Charge per sample	$25	$40	$60