UNF Department of Chemistry - Analytical Services
|
Dr. Nelson Zhao
Instrumentation Facility Manager
Phone: (904) 620-1962
E-mail: nelson.zhao@unf.edu
|
The Analytical Instrumentation Facility houses a number of advanced analytical instruments which can be used to analyze numerous samples for you. Our instruments include NMR, FTIR (Solid and Liquid), UV-Vis, AA, GC, GC/MS, and XRD.
Our services are available at reasonable prices. Whether it is a simple sample analysis, method development, or a more complicated structural elucidation, quality work is provided in a timely fashion.
Click the instrument below for rate information. The charges are on a per sample or per hour basis depending on the instrument involved. For special requests such as NMR data interpretations, analyses requiring the use of several instruments, complex mixture analysis, etc., please contact Nelson Zhao at (904) 620-1962 or by email at nelson.zhao@unf.edu
-
The NMR lab is equipped with a Agilent VNMRS 500 MHz Nuclear Magnetic Resonance
instrument.
Solution Probes:
-
1H-19F/15N-31P 5 mm PFG AutoX Dual Broadband
Probe for 1H, 19F, as well as other nuclei in the resonance
frequency range between 50 MHz (15N) and 202 MHz (31P).
-
1H-19F{13C} 5mm Triple resonance PFG probe; indirect
detection with high sensitivity for 1H and 19F.
Both probes have VT capability between -80°C and +120°C. In addition to 1D 1H,
19F, 13C, 31P, 29Si NMR experiments, the
instrument can acquire APT, DEPT, and 2D experiments such as COSY, TOCSY, NOESY, HSQC, and
HMBC.
Rates (per sample)
|
Charge per sample
|
On Campus
|
Off Campus (academic)
|
Industry
|
|
1H
|
$25 |
$40 |
$60 |
|
13C/29Si
|
$40 |
$55 |
$90 |
|
19F
|
$25 |
$40 |
$60 |
|
31P
|
$40 |
$55 |
$90 |
|
APT
|
$40 |
$60 |
$90 |
|
DEPT
|
$50 |
$70 |
$100 |
|
COSY
|
$40 |
$60 |
$80 |
|
TOCSY
|
$50 |
$70 |
$100 |
|
HSQC
|
$60 |
$100 |
$120 |
|
HMBC
|
$100 |
$150 |
$170 |
Solid State NMR - Please inquire
-
Available Instruments:
- Perkin-Elmer Spectrum BX (with liquid attenuated total reflectance (ATR) accessory)
- Perkin-Elmer Spectrum One (with solid attenuated total reflectance (ATR) accessory)
- Shimadzu IRAffinity-1 FTIR
IR Service Rates (per sample)
| Charge Per Sample |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge 1 hour.
Perkin Elmer Spectrum One FTIR
Perkin Elmer Spectrum BX FTIR
-
Perkin-Elmer Lambda 35 UV-Visible spectrophotometer can be used to perform quantitation,
spectral scans, and kinetic analysis in the ultraviolet (UV) to visible wavelength range
(190 - 850 nm).
Rates*
| Charge per hour |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge is 1 hour
Perkin Elmer Lambda 35 UV-Vis
-
The department is equipped with a Perkin Elmer AAnalyst 800 instrument for metals analysis. There are many Hollow Cathode Lamps (HCL) and Electrodeless Discharge Lamps (EDL) ready for metal ion analyses. They include Calcium, Iron, Magnesium, Manganese, Copper, Aluminum, Chromium, Zinc, Lead, Antimony, Cadmium, Selenium, Tin, and Arsenic. Please call Nelson Zhao at (904)620-1962 or by email at nelson.zhao@unf.edu for other metal analyses.
Rates*
| Charge per hour |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge is 1 hour
Perkin Elmer AAnalyst 800 AA
-
Available Instruments:
- Perkin Elmer Clarus 500 GC with FID
- Agilent HP5890 GC with FID/ECD (dual column option)
Rates*
| Charge per hour |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge is 1 hour
If method development is required, please contact Nelson Zhao at (904) 620-1962 or by email at nelson.zhao@unf.edu for rates.
Perkin Elmer Clarus 500GC
-
Available Instruments:
- Varian CP-3800 GC and Saturn 2200 GC/MS system
- Agilent HP5890 GC and HP5972 MS system
Rates*
| Charge per hour |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge is 1 hour
If method development is required, please contact Nelson Zhao at (904) 620-1962 or by email at nelson.zhao@unf.edu for quotes.
Varian CP-3800 and Saturn 2200 GC/Ms
-
Available Instruments:
- Rigaku Ultima III Powder Diffractometer
Rates*
| Charge per hour |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge is 1 hour
-
Available Instruments:
- Quanta Master 30 PTI Spectrofluorometer with high-power Xe flash lamp
Rates:
| Charge per hour |
| On Campus |
$40 |
| Off Campus (Academic) |
$60 |
| Industry |
$80 |
*minimum charge 1 hour
